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文章编号: 1672-6987(2020)05-0074-07; DOI: 10.16351/j.1672-6987.2020.05.010
王鹰1, 李成栋1*, 周熠智2
(1.青岛科技大学 材料科学与工程学院,山东 青岛 266042; 2.山东东岳化工集团,山东 淄博 256401)
摘要: 探索了一种采用熔体法原位制备含MgAl2O4尖晶石相的Al-Mg中间合金新工艺。采用金相显微镜(OM)、X射线衍射(XRD)、扫描电子显微镜(SEM)、X-射线能谱仪(EDS)等检测手段,研究了Al-Mg中间合金及其对8079铝合金晶粒大小及组织形貌和尺寸的影响。结果表明,Al-Mg中间合金对8079铝合金组织有明显的细化作用。显著改善了8079铝合金组织形貌,大尺寸的树枝晶碎裂成为短杆状等轴晶;当Al-Mg中间合金的添加量为3%,α-Al的最小尺寸可达30 μm。
关键词: 8079铝合金; MgAl2O4尖晶石; Al-Mg中间合金; 晶粒细化
中图分类号: TG 13文献标志码: A
引用格式: 王鹰, 李成栋, 周熠智. 原位反应制备新型Al-Mg中间合金及其对8079铝合金组织的细化作用\[J\]. 青岛科技大学学报(自然科学版), 2020, 41(5): 74-80.
WANG Ying, LI Chengdong, ZHOU Yizhi. Study on microstructure refinement of 8079 aluminum alloy by in-situ reaction preparation of new Al-Mg master alloy\[J\]. Journal of Qingdao University of Science and Technology(Natural Science Edition), 2020, 41(5): 74-80.
Study on Microstructure Refinement of 8079 Aluminum Alloy
by In-situ Reaction Preparation of New Al-Mg Master Alloy
WANG Ying1, LI Chengdong1, ZHOU Yizhi2
(1.College of Materials Science and Engineering, Qingdao University of Sicence and Technology,
Qingdao 266042,China;2.Shandong Dongyue Federation, Zibo 256401,China)
Abstract: In this paper, a new process of Al-Mg master alloy containing in-situ MgAl2O4 particles was explored by melt method.The Al-Mg master alloy was characterized by optical microscopy (OM), X-ray diffraction (XRD), scanning electron microscopy (SEM), and X-ray energy dispersive spectroscopy (EDS). The effects of Al-Mg master alloy on the grain size were observed. The results show that the Al-Mg master alloy has obvious refinement effect. The Al-Mg master alloy can significantly refine the microstructure of 8079 aluminum alloy. Large-sized dendrites are broken into short rod-like equiaxed crystals. When the Al-Mg master alloy is added, the grains can be remarkably refined, and the minimum size of α-Al can be 30 μm.
Key words: 8079 aluminum alloy; MgAl2O4 spinel; Al-Mg master alloy; grain refinement
收稿日期: 2019-08-01
基金项目: 国家自然科学基金项目(51672145).
作者简介: 王鹰(1990—),男,硕士研究生.*通信联系人.