PDF全文下载:2011030268
曹俊伟, 王宝源, 钟惠民*
(青岛科技大学 化学与分子工程学院,山东 青岛 266042)
摘要: 通过溶剂萃取、硅胶柱色谱及凝胶色谱等分离手段从虎尾草Lysimachia Barystachys中分离得到6个化合物。经IR、NMR等波谱技术,确定其化学结构分别为:槲皮素、山奈酚、山奈酚-3-O-β-D-半乳糖苷、槲皮素-3-O-β-D-葡萄糖苷、β-谷甾醇、β-胡萝卜苷。其中化合物山奈酚-3-O-β-D-半乳糖苷、槲皮素-3-O-β-D-葡萄糖苷、β-胡萝卜苷为首次从该植物中分离得到。
关键词: 虎尾草; 化学成分; 色谱技术
中图分类号: Q 946文献标志码: A
Studies on the Chemical Constituents of Lysimachia Barystachys
CAO Jun-wei, WANG Bao-yuan, ZHONG Hui-min
(College of Chemistry and Molecular Engineering,Qingdao University of Science and Technology,Qingdao 266042,China)
Abstract:Six compounds were isolated by using solvent extraction, silica gel column chromatography and gel chromatography from Lysimachia barystachys. Their structures were identified as following based on IR and NMR spectrum: quercetin, kaempferol, kaempferol-3-O-β-D-galactopyranoside, quercetin-3-O-β-D-glucopyranoside, β-sitosterol, anddaucosterol. Kaempferol-3-O-β-D-galactopyranoside, quercetin-3-O-β-D-glucopyranoside, anddaucosterol were isolated for the first time from this plant.
Key words: Lysimachia barystachys; chemical constituents; chromatographies
收稿日期: 2010-10-10
作者简介: 曹俊伟(1985—),女,硕士研究生.*通信联系人.