全文下载: 20240609.pdf
文章编号: 1672-6987(2024)06-0073-06; DOI: 10.16351/j.1672-6987.2024.06.009
马小龙1,2, 周龙海1, 曹奕晨2, 刘开强1, 刘城昊2, 陈昊1,2, 王爱娟2*(1.西安诺博尔稀贵金属材料股份有限公司,陕西 西安 710065; 2.西安理工大学 材料科学与工程学院, 陕西 西安 710048)
摘要: 以90% 变形量的Pd40Cu 合金为研究对象,进行550 ℃/60 min,650 ℃/30 min,650 ℃/60 min的热处理,分析热处理过程中的再结晶行为及组织的演变规律。结果表明:Pd40Cu 合金在550 ℃/60 min 热处理后为带状组织,650 ℃/30 min 热处理后为完全再结晶且晶粒细小、分布均匀;随着保温时间的增加,再结晶晶粒发生明显的长大。热处理后, Pd40Cu 合金再结晶Cube 织构的含量很少,S 型织构和Brass 织构的含量相对来说较多。由于大变形量下合金内部的储存能较高,在 550 ℃热处理后,大部分晶粒已完成再结晶转变,在升高温度的过程中晶粒尺寸增加,而织构的含量没有发生较大的变化。
关键词: Pd40Cu 合金箔; 组织演变; 织构; 缺陷
中图分类号: TG 146.3+2文献标志码: A
引用格式: 马小龙, 周龙海, 曹奕晨, 等. 90%变形量的Pd40Cu合金在热处理过程中的组织演变[J]. 青岛科技大学学报(自然科学版), 2024, 45(6): 73-78.
MA Xiaolong, ZHOU Longhai, CAO Yichen, et al. Microstructure evolution of Pd40Cu alloy with 90% deformation during heat treatment[J]. Journal of Qingdao University of Science and Technology(Natural Science Edition), 2024, 45(6): 73-78.
Microstructure Evolution of Pd40Cu Alloy with 90%
Deformation During Heat Treatment
MA Xiaolong1,2, ZHOU Longhai1, CAO Yichen2, LIU Kaiqiang1,
LIU Chenghao2, CHEN Hao1, WANG Aijuan2
(1.Xi′an Noble Rare Metal Materials Co. Ltd., Xi′an 710065, China;
2.School of Materials Science and Technology, Xi′an University of Technology, Xi′an 710048, China)
Abstract: 90% deformed Pd40Cu alloy was annealed at 550 ℃/60 min, 650 ℃/30 min, 650 ℃/60 min. Recrystallization behavior and microstructure evolution during the annealing process were analyzed. The results show that the microstructure of Pd40Cu alloy is banded after annealing at 550 ℃/60 min, and the recrystallized grains are completely recrystallized after annealing at 650 ℃/30 min, and the recrystallized grains are small and evenly distributed. With the increase of holding time, the recrystallized grains grow obviously. After annealing, the Cube texture content in the recrystallization annealing of Pd40Cu alloy is very small, while the S-shaped texture and Brass texture content are relatively large. Due to the higher storage energy of large deformation, most of the recrystallized grains finish nucleation after annealing at 550 ℃, and only the grain growth process is in the process of increasing the temperature. The texture content did not change greatly.
Key words: Pd40Cu alloy foil; microstructure evolution; texture; defects
收稿日期: 2023-12-10
基金项目: 秦创原产业创新聚集区“四链”融合项目(2024CY-JJQ-81).
作者简介: 马小龙(1980—),男,高级工程师.*通信联系人.