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文章编号： 16726987（2019）01005304； DOI： 10.16351/j.16726987.2019.01.009
孙璐璐， 刘保强， 建方方*
(青岛科技大学 材料科学与工程学院，山东 青岛 266042)
摘要： 近年来，新兴的二维过渡金属硫族化合物（TMDs)材料一直是研究的热点。其中，二硫化钼（MoS2）的优异性能引起了人们的广泛关注。TMDs材料制备方法多样，然而所制备的材料都不可避免地存在着晶界缺陷。晶界的存在会对材料的性能产生很大影响，人们通过各种方法来研究它。传统的研究方法存在很多局限性如操作复杂、耗时、引入人为缺陷等。这里报道了一种通过光学显微镜直接观察MoS2晶界的方法：通过化学气相沉积法（CVD）成功制备了大面积单层MoS2，将铜沉积在MoS2的表面在光学显微镜下可以直接观察到MoS2的晶界，实现了对其晶界的原位光学显微观测。同时，借助扫描电子显微镜（SEM）等进一步证实了该方法的简便可靠性。
关键词： 化学气相沉积； 二硫化钼； 晶界； 光学显微镜； 原位观测
中图分类号： O 063 文献标志码： A引用格式：孙璐璐， 刘保强， 建方方. 单层二硫化钼的制备及其晶界的原位光学表征\[J\]. 青岛科技大学学报（自然科学版）， 2019， 40（1）： 5356.
SUN Lulu, LIU Baoqiang, JIAN Fangfang. Preparation of single layer molybdenum disulfide and insitu optical characterization of grain boundary\[J\]. Journal of Qingdao University of Science and Technology（Natural Science Edition), 2019, 40(1)： 5356.
Preparation of Single Layer Molybdenum Disulfide and Insitu Optical Characterization of Grain Boundary
SUN Lulu, LIU Baoqiang, JIAN Fangfang
(College of Materials Science and Engineering, Qingdao University of Science and Technology, Qingdao 266042, China)
Abstract: In recent years, there is a hot topic of the emerging twodimensional transition metal chalcogenides (TMDs). Two dimensional molybdenum disulfide (MoS2) has attracted a lot of attentions. There are many ways to prepare this material but the grain boundaries are inevitable. The grain boundaries have a great influence on their properties and people have been studying this field through various means. In traditional, studying the grain boundaries has many disadvantages, such as complex operations, time consuming and artificial defects. Here we report a simple method for the visualization of large GBs in MoS2. Copper was deposited on the MoS2 grown by chemical vapor deposition（CVD）, and then the GBs could be observed by optical microscope. At the same time, the simple reliability of the method was confirmed by scanning electron microscope.
Key words:chemical vapor deposition; molybdenum disulfide; grain boundary; optical microscopic; insitu characterization
收稿日期： 20180108
基金项目： 国家自然科学基金项目（21573253）.
作者简介： 孙璐璐(1993—)，女，硕士研究生.*通信联系人.
